Triple Lab Showdown - HPL Premium Plus PCMO 0W-30

I got an answer from LSJr on why the lab SD uses reports much higher levels of molybdenum than others. He said SD's lab uses RDE vs ICP, without saying ICP is the method used by other specific labs.

"Most labs use the ICP method, which only sees particles up to about 5 microns. We use the RDE method which can detect particles up to about 10 microns. Because of that, Molybdenum levels are different between the methods due to Molybdenum forming platelets of various sizes."

In this article discussing Molybdenum disulphide as an oil additive, they mention "Molybdenum disulphide takes the form of microscopic hexagonal platelets, with several molecules making up each platelet."

Here is a link to a Philips 66 paper on "Understanding Differences in Elemental Analysis Methods" which talks about ICP vs RDE. Their summary pretty much says it all:

"If you are relying on one method at a lab for your used oils, then you should also use the same method at the same lab for the new oil reference for proper comparison. Finally, one elemental analysis report should not be taken as absolute, instead trends in the data should be observed over a historical period while comparing to a new oil reference."


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That is good to know. Thanks for reaching out to get answers. Also nice to know you received a reasonable response.
 
Good grief, Blackstone really needs to get their act together 🤦‍♂️
Could not agree with you more as usual. I don't think you could get me to use Blackstone. Some of these oil analysis institutions are just a hair or two away from being pathetic. They just haven't ever tested a really really good oil so they don't know how to handle it. It just goes to show that sometimes a basic oil analysis is fine but in certain circumstances and with certain higher quality higher end material the money we tried to spend to get an answer only left us with twice as many questions remaining.
 
That is good to know. Thanks for reaching out to get answers. Also nice to know you received a reasonable response.
Lake's been very responsive to follow-up emails, and I've had many. When looking for an oil for the Audi, he cautioned me about using the Ravenol VSE in a DI, turbocharged engine due to the high levels of calcium and sodium.

I'll continue to use SD and pay closer attention to all the fields when a report arrives and immediately let him know if there are discrepancies. Hopefully he'll get better at catching himself. No doubt with 6.2L issues, he's busier than ever.
 
Lake's been very responsive to follow-up emails, and I've had many. When looking for an oil for the Audi, he cautioned me about using the Ravenol VSE in a DI, turbocharged engine due to the high levels of calcium and sodium.

I'll continue to use SD and pay closer attention to all the fields when a report arrives and immediately let him know if there are discrepancies. Hopefully he'll get better at catching himself. No doubt with 6.2L issues, he's busier than ever.

Thanks for following up on that. I would also like to know why SD fuel dilution numbers are only 30-50% as high vs OA/Polaris UOA’s when both labs use gas chromatography (~1% vs ~3%). I’ve only sent 2 UOA’s to both labs so far though. I’m planning to send my next few UOA samples to SD, OA, and wearcheck to see the fuel dilution numbers for comparison. I paid Wearcheck extra to ensure they will do the GC test, which they normally omit if the viscosity is close to their expected values.
 
IMO only if they're comparing from two different labs or more.
A few PPM is still only a few PPM. You’d need dozens of UOAs all at exactly the same number for a new incoming UOA that was a few PPM different to indicate anything at all, and even then it’s only minimally relevant unless it is off so far that it’s outside of the standard deviation of the measurement device’s accuracy.

I personally don’t even blink until the differences are double digits, and repeat over a least two consecutive UOAs.
 
Lake's been very responsive to follow-up emails, and I've had many. When looking for an oil for the Audi, he cautioned me about using the Ravenol VSE in a DI, turbocharged engine due to the high levels of calcium and sodium.

I'll continue to use SD and pay closer attention to all the fields when a report arrives and immediately let him know if there are discrepancies. Hopefully he'll get better at catching himself. No doubt with 6.2L issues, he's busier than ever.
Now that you have to question the veracity of the report, how are you supposed to feel
comfortable with any of the answers they provide? It’s not like you can guess which ones they actually got correct this time.

That’s one of the good, general reasons why a specific PPM result isn’t a bright idea to rely on, and exactly why a UOA is the correct tool to check viscosity, contamination, and BN/AN levels…. Not compare wear metals.
 
Now that you have to question the veracity of the report, how are you supposed to feel
comfortable with any of the answers they provide? It’s not like you can guess which ones they actually got correct this time.
I feel like I should be lying on a couch and writing a big check at the end of the session. Oh wait, I am writing a big check. Now I need a nap.
 
I found it interesting that the manufacturer of a new unleaded fuel for piston airplane engines was using blackstone anlaysis to assess the relative suitability of their fuel compared to the legacy leaded fuels. Granted they had to use engine teardowns and physically measure parts wear to gain certification for their fuel, but they were still doing oil analysis.

 
A few PPM is still only a few PPM. You’d need dozens of UOAs all at exactly the same number for a new incoming UOA that was a few PPM different to indicate anything at all, and even then it’s only minimally relevant unless it is off so far that it’s outside of the standard deviation of the measurement device’s accuracy.

I personally don’t even blink until the differences are double digits, and repeat over a least two consecutive UOAs.
OP shows more than just a few ppm. Lab variance is real & as stated different labs tests can have wildly different numbers. Best to stick with one lab & my post was to say lab variance is going to happen especially across different labs and showing others this post will only confirm that. Yes, small PPM differences from a different or same lab isn't an issue though.
 
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